diff --git a/cif_pow.dic b/cif_pow.dic index fe53c72..20ce5d2 100644 --- a/cif_pow.dic +++ b/cif_pow.dic @@ -2621,7 +2621,7 @@ save_PD_CALIB_DETECTED_INTENSITY _definition.id PD_CALIB_DETECTED_INTENSITY _definition.scope Category _definition.class Loop - _definition.update 2023-01-21 + _definition.update 2025-06-27 _description.text ; This section defines the parameters used for the intensity calibration of @@ -2646,11 +2646,70 @@ save_PD_CALIB_DETECTED_INTENSITY ; _name.category_id PD_GROUP _name.object_id PD_CALIB_DETECTED_INTENSITY + _category_key.name '_pd_calib_detected_intensity.detector_id' loop_ - _category_key.name - '_pd_calib_detected_intensity.detector_id' - '_pd_calib_detected_intensity.id' + _description_example.case + _description_example.detail +; + _audit_dataset.id cb6a263b-c573-4ec3-848e-cfa7e44f3ec6 + + loop_ + _pd_calib_detected_intensity.detector_id + _pd_calib_detected_intensity.detector_response + _pd_calib_detected_intensity.detector_response_su + _pd_calib_detected_intensity.diffractogram_id + _pd_calib_detected_intensity.phase_id + A 1 . DIFFRACTOGRAM_A 676A + B 1.0350 0.0006 DIFFRACTOGRAM_B 676A +; +; + The two detectors, A and B, have responses of 1 and 1.035, + respectively, meaning that their measured intensities must be divided + by these values to retreive their true values. These response values + were derived from an analysis of the diffraction patterns + DIFFRACTOGRAM_A and DIFFRACTOGRAM_B, both of which contain the phase + 676A. +; +; + loop_ + _pd_calib_detected_intensity.detector_id + _pd_calib_detected_intensity.detector_response + _pd_calib_detected_intensity.special_details + 1_4913c6ed 1 'Scanned through direct beam.' + 2_4913c6ed 0.973 'Scanned through direct beam.' + 3_4913c6ed 0.997 'Scanned through direct beam.' + 4_4913c6ed 1.039 'Scanned through direct beam.' +; +; + A multi-detector system was scanned through the direct beam to + calibrate the response of each detector to a constant-intensity + source. The measured intensity derived from each detector must be + divided by the given response to obtain the actual value. No + diffraction pattern or phase was involved in the derivation of the + response values. +; +; + _audit_dataset.id cb6a263b-c573-4ec3-848e-cfa7e44f3ec6 + _pd_diffractogram.id APATTERN + + loop_ + _pd_data.point_id + _pd_meas.detector_id + _pd_meas.2theta_scan + _pd_meas.intensity_total + _pd_proc.intensity_total + 1 A 10.00 1243.42(47) 1243.42(47) + 2 B 10.01 1364.36(57) 1318.22(94) + 3 A 10.02 1324.35(87) 1324.35(87) + 4 B 10.03 1298.36(74) 1254.45(102) + #... +; +; + The detector responses of 1 and 1.035 for detectors A and B given + in the first example have been applied to the raw measurements of + APATTERN to give processed intensities ready for analysis. +; save_ @@ -2660,11 +2719,8 @@ save_pd_calib_detected_intensity.detector_id _definition.update 2023-06-09 _description.text ; - A code which identifies the detector or channel number in a - position-sensitive, energy-dispersive or other multiple-detector - instrument for which the individual instrument geometry is being - defined. This code should match the code name used for - _pd_instr_detector.id. + A code which identifies the detector to which the response is being defined. + This code should match the code name used for _pd_instr_detector.id. ; _name.category_id pd_calib_detected_intensity _name.object_id detector_id @@ -2744,24 +2800,6 @@ save_pd_calib_detected_intensity.diffractogram_id save_ -save_pd_calib_detected_intensity.id - - _definition.id '_pd_calib_detected_intensity.id' - _definition.update 2023-01-21 - _description.text -; - A code to uniquely identify each intensity calibration. -; - _name.category_id pd_calib_detected_intensity - _name.object_id id - _type.purpose Key - _type.source Assigned - _type.container Single - _type.contents Text - _enumeration.default . - -save_ - save_pd_calib_detected_intensity.phase_id _definition.id '_pd_calib_detected_intensity.phase_id' @@ -13677,6 +13715,9 @@ save_ Added _pd_meas_overall.step_count_time. + Removed _pd_calib_detected_intensity.id as data item and category key + of PD_CALIB_DETECTED_INTENSITY. + Update PD_INSTR and PD_INSTR_DETECTOR descriptions. Added _pd_instr.radiation_id and _pd_instr_detector.instr_id.