Skip to content
Merged
Changes from all commits
Commits
File filter

Filter by extension

Filter by extension

Conversations
Failed to load comments.
Loading
Jump to
Jump to file
Failed to load files.
Loading
Diff view
Diff view
95 changes: 68 additions & 27 deletions cif_pow.dic
Original file line number Diff line number Diff line change
Expand Up @@ -2621,7 +2621,7 @@ save_PD_CALIB_DETECTED_INTENSITY
_definition.id PD_CALIB_DETECTED_INTENSITY
_definition.scope Category
_definition.class Loop
_definition.update 2023-01-21
_definition.update 2025-06-27
_description.text
;
This section defines the parameters used for the intensity calibration of
Expand All @@ -2646,11 +2646,70 @@ save_PD_CALIB_DETECTED_INTENSITY
;
_name.category_id PD_GROUP
_name.object_id PD_CALIB_DETECTED_INTENSITY
_category_key.name '_pd_calib_detected_intensity.detector_id'

loop_
_category_key.name
'_pd_calib_detected_intensity.detector_id'
'_pd_calib_detected_intensity.id'
_description_example.case
_description_example.detail
;
_audit_dataset.id cb6a263b-c573-4ec3-848e-cfa7e44f3ec6

loop_
_pd_calib_detected_intensity.detector_id
_pd_calib_detected_intensity.detector_response
_pd_calib_detected_intensity.detector_response_su
_pd_calib_detected_intensity.diffractogram_id
_pd_calib_detected_intensity.phase_id
A 1 . DIFFRACTOGRAM_A 676A
B 1.0350 0.0006 DIFFRACTOGRAM_B 676A
;
;
The two detectors, A and B, have responses of 1 and 1.035,
respectively, meaning that their measured intensities must be divided
by these values to retreive their true values. These response values
were derived from an analysis of the diffraction patterns
DIFFRACTOGRAM_A and DIFFRACTOGRAM_B, both of which contain the phase
676A.
;
;
loop_
_pd_calib_detected_intensity.detector_id
_pd_calib_detected_intensity.detector_response
_pd_calib_detected_intensity.special_details
1_4913c6ed 1 'Scanned through direct beam.'
2_4913c6ed 0.973 'Scanned through direct beam.'
3_4913c6ed 0.997 'Scanned through direct beam.'
4_4913c6ed 1.039 'Scanned through direct beam.'
;
;
A multi-detector system was scanned through the direct beam to
calibrate the response of each detector to a constant-intensity
source. The measured intensity derived from each detector must be
divided by the given response to obtain the actual value. No
diffraction pattern or phase was involved in the derivation of the
response values.
;
;
_audit_dataset.id cb6a263b-c573-4ec3-848e-cfa7e44f3ec6
_pd_diffractogram.id APATTERN

loop_
_pd_data.point_id
_pd_meas.detector_id
_pd_meas.2theta_scan
_pd_meas.intensity_total
_pd_proc.intensity_total
1 A 10.00 1243.42(47) 1243.42(47)
2 B 10.01 1364.36(57) 1318.22(94)
3 A 10.02 1324.35(87) 1324.35(87)
4 B 10.03 1298.36(74) 1254.45(102)
#...
;
;
The detector responses of 1 and 1.035 for detectors A and B given
in the first example have been applied to the raw measurements of
APATTERN to give processed intensities ready for analysis.
;

save_

Expand All @@ -2660,11 +2719,8 @@ save_pd_calib_detected_intensity.detector_id
_definition.update 2023-06-09
_description.text
;
A code which identifies the detector or channel number in a
position-sensitive, energy-dispersive or other multiple-detector
instrument for which the individual instrument geometry is being
defined. This code should match the code name used for
_pd_instr_detector.id.
A code which identifies the detector to which the response is being defined.
This code should match the code name used for _pd_instr_detector.id.
;
_name.category_id pd_calib_detected_intensity
_name.object_id detector_id
Expand Down Expand Up @@ -2744,24 +2800,6 @@ save_pd_calib_detected_intensity.diffractogram_id

save_

save_pd_calib_detected_intensity.id

_definition.id '_pd_calib_detected_intensity.id'
_definition.update 2023-01-21
_description.text
;
A code to uniquely identify each intensity calibration.
;
_name.category_id pd_calib_detected_intensity
_name.object_id id
_type.purpose Key
_type.source Assigned
_type.container Single
_type.contents Text
_enumeration.default .

save_

save_pd_calib_detected_intensity.phase_id

_definition.id '_pd_calib_detected_intensity.phase_id'
Expand Down Expand Up @@ -13677,6 +13715,9 @@ save_

Added _pd_meas_overall.step_count_time.

Removed _pd_calib_detected_intensity.id as data item and category key
of PD_CALIB_DETECTED_INTENSITY.

Update PD_INSTR and PD_INSTR_DETECTOR descriptions.

Added _pd_instr.radiation_id and _pd_instr_detector.instr_id.
Expand Down